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Synthesis and Application of Super-Hydrophobic Titanosilicates Sphere
Author NameAffiliationE-mail
ZHOU Hui Department of Chemistry, Zhejiang University, Hangzhou 310027, China
College of Chemical and Biological Engineering, Zhejiang University, Hangzhou 310027, China
Hangzhou First Applied Material Co., Ltd., Hangzhou 311300, China 
 
LI Sha Key Laboratory of Chemical Utilization of Forestry Biomass of Zhejiang Province, Zhejiang A & F University, Hangzhou 311300, China  
XIAO Li-Ping Department of Chemistry, Zhejiang University, Hangzhou 310027, China lpxiao@zju.edu.cn 
FAN Jie Department of Chemistry, Zhejiang University, Hangzhou 310027, China  
ZHENG Xiao-Ming Department of Chemistry, Zhejiang University, Hangzhou 310027, China  
Abstract: Layered organo-titanosilicate materials with a micro sphere morphology (denoted as ms-LOTS) were synthesized via the aerosol-assisted self-assembly (AASA) method. The morphology and materials' structure of ms-LOTS was characterized by SEM, XRD and FT-IR. The temperature and concentration play an important role in catalytic activity. The ms-LOTS with a uniform sphere size of 2~4 μm were successfully prepared by the optimization of synthetic condition (350℃ and low concentration). At room temperature, ms-LOTS show improved catalytic performance in the epoxidation of cyclohexene.
Keywords: titanosilicate  super-hydrophobicity  organo-inorgano hybrid  micro sphere material
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ZHOU Hui,LI Sha,XIAO Li-Ping,FAN Jie,ZHENG Xiao-Ming.Synthesis and Application of Super-Hydrophobic Titanosilicates Sphere[J].Chinese Journal of Inorganic Chemistry,2018,34(6):1051-1058.
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Chinese Journal of Inorganic Chemistry