| 一种Λ型吡啶碘盐的合成和晶体结构 |
| Synthesis and Crystal Structure of a New Λ Type Pyridine Iodide |
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| 摘要: |
| 关键词: Λ型吡啶碘盐 合成 晶体结构 |
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| Abstract: A new Λ type pyriding iodide was synthesized by reaction of 4-picoline and methyl diiodide. The structure was characterized by elemental analysis, IR, UV and TG. The crystal structure of the title compound was determined by X-ray single crystal diffraction. The crystal belongs to monoclinic with space group C2/c, a=18.812(4)?, b=8.7816(6)?, c=10.3165(12)?, β=93.71(1), V=1700.7(4)?3, Z=4. In the molecule, two 4-picoline molecules are bonded by -CH2 group to form Λ type pyridine salt. CCDC: 180871. |
| Keywords: Λ type pyriding iodide synthesig crystal structure |
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| 张颖,吴杰颖,于文涛,田玉鹏,蒋民华.一种Λ型吡啶碘盐的合成和晶体结构[J].无机化学学报,2002,18(10):1020-1022. |
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