硬脂酸法制备超细K2La2Ti3O10及其酸交换性质研究
Preparation of Ultrafine K2La2Ti3O10 by Stearic Acid Method and Study on its Acid-exchanging Property
作者单位
张莉莉 南京理工大学材料化学实验室南京 210094 
杨 娟 江苏大学材料科学与工程学院镇江 212013 
张维光 南京理工大学材料化学实验室南京 210094 
陆路德 南京理工大学材料化学实验室南京 210094 
杨绪杰 南京理工大学材料化学实验室南京 210094 
汪 信 南京理工大学材料化学实验室南京 210094 
摘要: 
关键词: 硬脂酸法 K2La2Ti3O10 酸交换 剥离
基金项目: 
Abstract: A new stearic acid method(SAM) has been used to prepare ultrafine K2La2Ti3O10 nanocrystalline. Each state of synthesis process was followed by the use of FT-IR analysis. The resulting materials have been characterized by means of XRD, TEM, BET surface area analysis. The acid-exchanging property of the obtained product was also studied. The experimental results showed that comparing with the product of traditional solid-state reaction, the particle size of the K2La2Ti3O10 synthesized by SAM is greatly reduced, BET surface area is high(more than 11.83m2·g-1) and has different acid-exchanging properties. It can be easily exfoliated in 2mol·L-1 HNO3 so-lution.
Keywords: stearic acid method layered lanthanum titanate acid-exchanging exfoliation
 
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张莉莉,杨 娟,张维光,陆路德,杨绪杰,汪 信.硬脂酸法制备超细K2La2Ti3O10及其酸交换性质研究[J].无机化学学报,2003,19(11):1217-1221.
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