凝胶网格沉淀法制备MgO纳米晶
Preparation of MgO Nanocrystalline by Gel-network Precipitation Method
作者单位
周建国 河南师范大学化学与环境科学学院新乡 453007
兰州大学化学化工学院兰州 730000 
汪应灵 河南师范大学化学与环境科学学院新乡 453007 
赵凤英 河南师范大学科技与社会研究所新乡 453007 
李振泉 河南师范大学化学与环境科学学院新乡 453007 
高世扬 河南师范大学化学与环境科学学院新乡 453007
兰州大学化学化工学院兰州 730000 
摘要: 
关键词: MgO  纳米晶  凝胶网格沉淀法
基金项目: 
Abstract: Monodispersed spherical MgO nanocrystallites were successfully prepared by a novel gel-network precipitation process. The face-centred cubic samples were with narrow size distribution of 10~15 nm. The formation process and structure of MgO nanocrystallites were investigated by means of TG-DTA, FTIR, XRD and TEM. The results show that the particle sizes are related to the network structure of gelatin, not only can the shapes and sizes of nanocrystallites be controlled, but the aggregation and agglomeration can be prevented by gel-network. The products have smaller particle size and better homogeneity.
Keywords: MgO  nanocrystalline  gel-network precipitation method
投稿时间:2004-05-12 修订日期:2004-11-10
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周建国,汪应灵,赵凤英,李振泉,高世扬.凝胶网格沉淀法制备MgO纳米晶[J].无机化学学报,2005,21(2):221-224.
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