| 选相原位法合成立方氮化硼的关键影响因素 |
| The Key Factors on in situ Synthesis of Cubic Boron Nitride |
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| 摘要: 利用选相原位法在水溶液中成功制备出了立方氮化硼晶体，对反应条件进行了优化。结果表明，利用选相原位法合成立方氮化硼的最佳实验条件是：反应压力为10.0 MPa，在氯离子加入下利用混合氮源进行反应。在该条件下得到了纯相的立方氮化硼晶体。 |
| 关键词: 水热法 立方氮化硼 选相原位合成 |
| 基金项目: |
| Abstract: Cubic boron nitride (c-BN) crystals have been synthesized in water solution using in situ phase-selective method. In order to improve the crystalline quality and the relative content of c-BN, the reaction conditions were optimized. The experimental results indicated that, the optimal reacting conditions for the method were: reaction under pressure of 10.0 MPa with Cl- addition and mixed nitrogen resource. |
| Keywords: hydrothermal method cubic boron nitride in situ phase-selective synthesis |
| 投稿时间：2004-10-25 修订日期：2005-01-13 |
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| 于美燕,崔得良,尹衍升,初蕾,孙峰.选相原位法合成立方氮化硼的关键影响因素[J].无机化学学报,2005,21(5):653-657. |
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