碳化硅纳米管的制备及表征
Synthesis and Characterization of Silicon Carbide Nanotubes
作者单位
陶德良 湖南工业大学绿色包装与生物纳米技术应用湖南省重点实验室, 株洲 412008 
谢征芳 国防科学技术大学航天与材料工程学院新型陶瓷纤维及其复合材料国防科技重点实验室, 长沙 410073 
何农跃 湖南工业大学绿色包装与生物纳米技术应用湖南省重点实验室, 株洲 412008 
摘要: 
关键词: 碳化硅纳米管  化学气相沉积  表征
基金项目: 
Abstract: Silicon carbide nanotubes (SiCNTs) were prepared by chemical vapor deposition (CVD). Methyltrichlorosilane (MTS) was selected as the SiC gaseous source and, ferrocence and thiophene as the catalyst and the cocatalyst, respectively. The influences of pyrolysis temperature, the content of catalyst and the cocatalyst, and the mole ratio between H2 and MTS, on the shape of the pyrolysis products were investigated, respectively. The products were characterized by SEM, EDX, XRD and HRTEM, respectively. Novel type of multi-walled SiCNTs, with 30~80 nm and 15~20 nm outer and inner diameters, respectively, were observed.
Keywords: silicon carbide nanotubes  chemical vapor deposition  characterization
 
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陶德良,谢征芳,何农跃.碳化硅纳米管的制备及表征[J].无机化学学报,2006,22(5):945-948.
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