水热法制备具有光滑表面的球形Y2O3∶Eu3+发光材料(英文)
Hydrothermal Synthesis of Spherical Y2O3∶Eu3+ Luminescent Materials with Smooth Surface
作者单位
刘桂霞 长春理工大学材料与化工学院长春 130022
中国科学院长春应用化学研究所稀土化学与物理重点实验室长春 130022 
洪广言 中国科学院长春应用化学研究所稀土化学与物理重点实验室长春 130022 
王进贤 长春理工大学材料与化工学院长春 130022 
董相廷 长春理工大学材料与化工学院长春 130022 
摘要: 
关键词: 球形Y2O3∶Eu3+  荧光粉  水热法  发光材料
基金项目: 
Abstract: The spherical Y2O3∶Eu3+ luminescent particles with size of 0.5~3 μm and smooth surface were synthesized by hydrothermal method. The resulted Y2O3∶Eu3+ precursors and the calcined particles were characterized by differential thermal analysis (DTA) and thermogravimetric (TG) analysis, X-ray diffraction (XRD), Fourier-transform IR spectroscopy (FTIR), scanning electron microscopy (SEM) and photoluminescence spectra (PL). FTIR, TG-DTA, XRD measurements show that the precursors are crystal with hydroxyl and carbonate group, and the pure cubic yttria is obtained after annealing above 700 ℃. The SEM images indicate that the Y2O3∶Eu3+ particles are in spherical shape and with smooth surface. PL analysis shows that the particles present characteristic red emission of Eu3+.
Keywords: spherical Y2O3∶Eu3+  phosphors  hydrothermal method  luminescent materials
 
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刘桂霞,洪广言,王进贤,董相廷.水热法制备具有光滑表面的球形Y2O3∶Eu3+发光材料(英文)[J].无机化学学报,2006,22(8):1535-1539.
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