微乳液法制备YF3∶Er纳米材料 |
Preparation of Er-doped YF3 Nanomaterials by Microemulsion |
|
摘要: |
关键词: 微乳液 稀土氟化物 红外荧光 上转换发光 |
基金项目: |
Abstract: Er-doped YF3 nanoparticles were prepared from quaternary microemulsions of cetyltrimethyl ammonium bromide, n-butanol, n-octane and water with oil to water(mass percent of ω(CTAB)=19.04%, ω(n-butanol)=15.24%, ω(n-octane)=51.40%. The nanofluorides were characterized by X-ray power diffraction and infrared fluorescence spectroscopy. The results of XRD are in agreement with the PDF#74-911 of YF3. The average grain size is about 30 nanometer as estimated by Scherrer Formula. ESEM images show that the diameter of BaF2∶Er3+ nanoparticles is 35 nm. The emission of infrared fluorescence spectroscopy of the predominant peak is located at 1 547 nm and the up-conversion optical properties measured with 980 nm laser diode show red and green emissions. |
Keywords: microemulsion rare-earth fluoride fluorescence infrared up-conversion luminescence |
|
摘要点击次数: 1579 |
全文下载次数: 2008 |
闫景辉,宋丽红,李中田,张海燕,张挥球.微乳液法制备YF3∶Er纳米材料[J].无机化学学报,2007,23(8):1432-1434. |
查看全文 查看/发表评论 下载PDF阅读器 |
Support information: |
|
|
|