微乳液法制备YF3∶Er纳米材料
Preparation of Er-doped YF3 Nanomaterials by Microemulsion
作者单位
闫景辉 长春理工大学化学与环境工程学院长春 130022 
宋丽红 长春理工大学化学与环境工程学院长春 130022 
李中田 长春理工大学化学与环境工程学院长春 130022 
张海燕 长春理工大学化学与环境工程学院长春 130022 
张挥球 长春理工大学化学与环境工程学院长春 130022 
摘要: 
关键词: 微乳液  稀土氟化物  红外荧光  上转换发光
基金项目: 
Abstract: Er-doped YF3 nanoparticles were prepared from quaternary microemulsions of cetyltrimethyl ammonium bromide, n-butanol, n-octane and water with oil to water(mass percent of ω(CTAB)=19.04%, ω(n-butanol)=15.24%, ω(n-octane)=51.40%. The nanofluorides were characterized by X-ray power diffraction and infrared fluorescence spectroscopy. The results of XRD are in agreement with the PDF#74-911 of YF3. The average grain size is about 30 nanometer as estimated by Scherrer Formula. ESEM images show that the diameter of BaF2∶Er3+ nanoparticles is 35 nm. The emission of infrared fluorescence spectroscopy of the predominant peak is located at 1 547 nm and the up-conversion optical properties measured with 980 nm laser diode show red and green emissions.
Keywords: microemulsion  rare-earth fluoride  fluorescence infrared  up-conversion luminescence
 
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全文下载次数:  2008
闫景辉,宋丽红,李中田,张海燕,张挥球.微乳液法制备YF3∶Er纳米材料[J].无机化学学报,2007,23(8):1432-1434.
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