通过β-FeOOH纳米棒无序聚集制备α-Fe2O3中空球 |
Preparation of α-Fe2O3 Hollow Spheres via Random Aggregation of β-FeOOH Nanorods |
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摘要: |
关键词: 氧化铁 氧化氢氧化铁 中空 溶剂热 无序聚集 |
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Abstract: The α-Fe2O3 hollow spheres have been synthesized through the random aggregation of β-FeOOH nanorods in the C2H5OH/H2O system. The phase transformation and the morphologies of the α-Fe2O3 hollow structure were investigated with XRD, SEM, TEM and selected area electron diffraction (SAED). These studies indicate that the second step is a dissolution-recrystallization process. Furthermore, the formation mechanism of the hollow spheres has been discussed. It is found that the presence of H2O in the reaction system is essential to the final formation of the hollow spheres. |
Keywords: α-Fe2O3 β-FeOOH hollow solvent-thermal random aggregation |
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俞海云,陈国柱,孙思修,印志磊,宋新宇.通过β-FeOOH纳米棒无序聚集制备α-Fe2O3中空球[J].无机化学学报,2007,23(12):2115-2118. |
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