| 杯[4]芳烃二肟酸-Cu(Ⅰ)配合物的设计与自组装合成 | |||||||||||||
| Design and Self-assembled Synthesis of Calix[4]-1,3-bis-oxime-Cu(Ⅰ) Complex | |||||||||||||
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| 关键词: 杯[4]芳烃 肟酸 铜配合物 自组装 | |||||||||||||
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| Abstract: Calix[4]-1,3-bis-oxime derivative 2 was prepared by ammonolysis of calix[4]-1,3-bis-esters with hydroxyl-amine. Further refluxing compound 2 with CuCl2·2H2O in ethanol, the calix[4]-1,3-bis-oxime-Cu+ complex 3 was pr-epared by self-assembled reaction. The structures of new compound and complex were confirmed by element analyses, IR, 1H NMR, MS, EPR and 1H-1H COSY spectrum. | |||||||||||||
| Keywords: calix[4]arene oxime Cu+ complex self-assembled | |||||||||||||
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| 杨发福,洪碧琼,郑小花,郭红玉,刘朝晖.杯[4]芳烃二肟酸-Cu(Ⅰ)配合物的设计与自组装合成[J].无机化学学报,2008,24(1):153-156. | |||||||||||||
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