水溶性荧光CdSe量子点的合成及其在指纹显现中的应用
Water-Soluble Fluorescent CdSe Quantum Dots: Synthesis and Application for Fingerprint Developing
作者单位
石志霞 北京化工大学理学院北京 100029 
王元凤 中国人民公安大学北京 100038 
刘建军 北京化工大学理学院北京 100029 
杨瑞琴 中国人民公安大学北京 100038 
左胜利 北京化工大学理学院北京 100029 
于迎春 北京化工大学理学院北京 100029 
摘要: 
关键词: CdSe量子点  水相合成  荧光  指纹显现
基金项目: 
Abstract: Water-soluble fluorescent CdSe quantum dots(QDs) were synthesized by using Se、Na2SO3 and CdCl2 as precursors and mercaptoacetic acid(TGA) as modifier. The effects of refluxing time and initial pH values of the reaction on the particle size and fluorescence intensity of CdSe QDs were studied. The XRD、HRTEM and fluorescent spectroscopy were employed to characterize these samples. It is found that CdSe QDs with crystalline size of 2~3 nm are homogeneously distributed in the organic matrix. The maximum fluorescence absorption and emission peak of CdSe QDs solution are at 450 nm and 562 nm, respectively. The fingerprint details on the surface of smooth objects were clearly developed with CdSe QDs solution under irradiation of UV lights.
Keywords: CdSe QDs  aqueous synthesis  fluorescence  fingerprint development
 
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石志霞,王元凤,刘建军,杨瑞琴,左胜利,于迎春.水溶性荧光CdSe量子点的合成及其在指纹显现中的应用[J].无机化学学报,2008,24(7):1186-1190.
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