| 纳米铂-纤维配合物(Pt(0)/AOCF)的制备及表征 |
| Preparation and Characterization of Nano-Pt(0)/AOCF Complex |
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| 摘要: |
| 关键词: Pt 偕胺肟纤维 配位 表征 |
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| Abstract: In this paper, spherical nano-sized particles on the amidoxime fiber surface have been successfully synthesized through a fast and easy coordination-reduction method. The particles have also been characterized by means of IR, SEM, XRD, XPS and EDS. The IR and XPS result shows that Pt(0) was chelated to fiber by chemical bonds. SEM shows that spherical Pt metal particles uniformly distributed on the fiber surface. The characteristic diffraction peaks at 39.99°, 46.48°, 67.90° of XRD pattern are in accordance with Pt standard card (PDF No.04-0802), which demonstrates the particles on the fiber surface is indeed Pt. EDS mapping has also fully proved this point. |
| Keywords: platinum fiber containing amidoxime groups coordination characterization |
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| 张 勇,吴之传,陶庭先,童 伟.纳米铂-纤维配合物(Pt(0)/AOCF)的制备及表征[J].无机化学学报,2009,25(7):1299-1303. |
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