| L-脯氨酸协助合成β-氢氧化镍和氧化镍花球及纳米三角片(英文) |
| L-Proline Assisted Synthesis of Flower-Like Microspheres and Triangular Nanosheets of β-Ni(OH)2 and NiO |
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| 摘要: 以NH3·H2O和NaOH作为沉淀剂，通过水热方法在180 ℃，L-脯氨酸作用下，分别合成出了β-Ni(OH)2花球和纳米三角片。XRD结果表明合成出的β-Ni(OH)2产物是六方相，透射电镜(TEM)和场发射电镜(FESEM)表明花球直径为1~2 μm，它是由厚15 nm，边长110 nm的三角片自组装形成的。对相应的β-Ni(OH)2前驱物在350 ℃空气下退火2 h，分别得到NiO花球和纳米三角片。 |
| 关键词: 氢氧化镍 氧化镍 合成 L-脯氨酸 |
| 基金项目: |
| Abstract: β-Ni(OH)2 flower-like microspheres and triangular nanosheets have been hydrothermally synthesized at 180 ℃ in the presence of L-proline using NH3·H2O and NaOH, respectively, as the precipitant. XRD patterns show that the as-prepared β-Ni(OH)2 products are hexagonal phase. TEM and FESEM images indicate that the flower-like microspheres with diameter of 1~2 μm are assembled from triangular nanosheets with thickness of 15 nm and edge length of 110 nm. NiO flower-like microspheres and triangular nanosheets can be obtained by calcining the β-Ni(OH)2 precursors at 350 ℃ for 2 h in air. |
| Keywords: nickel hydroxide nickel oxide synthesis L-proline |
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| 闫 岩,李海波,李敬发,潘 军,钱逸泰.L-脯氨酸协助合成β-氢氧化镍和氧化镍花球及纳米三角片(英文)[J].无机化学学报,2010,26(7):1141-1146. |
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