自堆积纤维状TS-1分子筛的常规水热合成
Self-stacked TS-1 Zeolite with Fibrous Morphology Prepared by Conventional Hydrothermal Method
作者单位
王 晔 南京工业大学化学化工学院材料化学工程国家重点实验室南京 210009 
李家栋 南京工业大学化学化工学院材料化学工程国家重点实验室南京 210009 
林 晓 南京工业大学化学化工学院材料化学工程国家重点实验室南京 210009 
摘要: 
关键词: 钛硅分子筛  形貌  层状堆积  常规水热合成
基金项目: 
Abstract: Self-stacked TS-1 crystals with fibrous morphology were prepared by conventional hydrothermal method. The synthesized samples were characterized by XRD, UV-Vis and SEM. The results show that TS-1 crystals with uniform shape and size are self-stacked on top of another along the crystallographic [010] direction to form the fibrous morphology under suitable hydrothermal synthesis conditions. Compared with silicalite, the Ti incorporated into the MFI framework induces stronger condensation of external hydroxyl groups of TS-1 crystals, resulting in formation of the self-stacked morphology.
Keywords: TS-1  morphology  self-stacking  conventional hydrothermal synthesis
 
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王 晔,李家栋,林 晓.自堆积纤维状TS-1分子筛的常规水热合成[J].无机化学学报,2010,26(9):1711-1714.
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