制备方法对AgInO2结构及光催化性能的影响 |
Effect of Preparation Method on Structure and Photocatalytic Performance of AgInO2 |
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摘要: 以离子交换法和“氟化异丙烯膜袋”水热法分别制备了AgInO2,利用XRD、低温氮吸附-脱附、SEM、紫外-可见漫反射光谱(UV-Vis diffuse reflection spectroscopy,DRS)和XPS对不同方法所得到的AgInO2进行了表征;以罗丹明B(RhB)和甲基橙(MO)为目标物,在可见光下考察了2种催化剂的光催化性能。结果表明,利用“氟化异丙烯膜袋”水热法制备的样品由于具有更好的结晶度,且在可见光区有更强的吸收,从而表现出了更好的可见光光催化活性(3 h降解RhB达94%。7 h降解MO达83%)。 |
关键词: 离子交换法 “氟化异丙烯膜袋”水热法 AgInO2 光催化 |
基金项目: |
Abstract: AgInO2 were prepared via ion exchange method and fluoro(ethylene-propylene) (FEP) facile hydrothermal method, respectively. The as-obtained samples were characterized by X-ray diffraction (XRD), N2-Adsorption, UV-Vis diffuse reflectance spectroscopy (DRS), scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS). The photocatalytic activity of the as-prepared catalysts was studied using dyes Rhodamine B (RhB) and Methyl Orange (MO)as the target degradation material under visible-light irradiation. The results indicate that the sample prepared by FEP hydrothermal method shows higher crystallinity and stronger absorption in visible light region, thus higher photocatalytic activity (94% of RhB was degraded in 3 h and 83% of MO was degraded in 7 h, respectively). |
Keywords: ion exchange method FEP hydrothermal method AgInO2 photocatalysis |
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郑华荣,陈永娟,董 辉,李朝晖.制备方法对AgInO2结构及光催化性能的影响[J].无机化学学报,2011,27(3):468-472. |
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