| 烧结反应对液相法制得FeWO4微米晶光催化性能的改性 |
| Effects of Annealing on Photocatalytic Properties of FeWO4 Microcrystals via Solution-Based Synthesis Method |
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| 摘要: 通过简单的液相法制得FeWO4微米晶，FeWO4微米晶于310℃、空气气氛条件下烧结，研究了烧结反应对FeWO4微米晶光催化性质的影响。烧结前后的样品通过X射线粉末衍射、扫描电子显微镜、透射电子显微镜、N2吸附-脱附、热重分析、红外分析和紫外-可见等分析方法加以表征。光催化实验证明烧结后其在降解罗丹明B溶液中表现出了较高活性，说明烧结反应有利于提高FeWO4的吸附与光催化性能。 |
| 关键词: FeWO4 烧结 光催化 |
| 基金项目: 安徽省自然科学基金（No.1508085QB46）资助项目。 |
| Abstract: FeWO4 microcrystals were fabricated through a simple solution-based route. Then, FeWO4 samples were annealed under the circumstance of air, with the temperature of 310℃, and the annealing process is firstly studied for its influence on FeWO4 microcrystals. The FeWO4 microcrystals, before and after annealing treatment, were characterized by XRD, SEM, TEM, N2 adsorption-desorption, TG, IR, and UV-Vis analysis. Annealed FeWO4 samples show highly active in degradation of rhodamine B (RhB). It reveals that the adsorptive and photocatalytic properties of FeWO4 microcrystals are probably enhanced through annealing treatment. |
| Keywords: FeWO4 annealing photo-catalysis |
| 投稿时间：2018-03-02 修订日期：2018-04-26 |
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| 杜泉岭,后浩,叶同奇,周红洋.烧结反应对液相法制得FeWO4微米晶光催化性能的改性[J].无机化学学报,2018,34(7):1373-1380. |
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