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Preparation and Electrocatalytic Performance of Flake Co9S8/ZnS/C Composites for Oxygen Evolution Reduction |
Author Name | Affiliation | E-mail | LI Zhi-Xue | College of Chemistry, Chemical Engineering and Environmental Engineering, Liaoning Shihua University, Fushun, Liaoning 113006, China | | REN Tie-Qiang | College of Chemistry, Chemical Engineering and Environmental Engineering, Liaoning Shihua University, Fushun, Liaoning 113006, China | | GENG Zhong-Xing | College of Chemistry, Chemical Engineering and Environmental Engineering, Liaoning Shihua University, Fushun, Liaoning 113006, China | | YANG Zhan-Xu | College of Chemistry, Chemical Engineering and Environmental Engineering, Liaoning Shihua University, Fushun, Liaoning 113006, China | zhanxuy@126.com |
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Abstract: The flake Co9S8/ZnS/C composites were prepared by solvothermal method, through using cobalt hexahydrate[Co(NO3)2·6H2O] as cobalt source, zinc hexahydrate nitrate[Zn(NO3)2·6H2O] as zinc source and 2,2'-thiodiacetic acid (C4H6O4S) as sulfur source. The flake Co9S8/ZnS/C composites structure and morphology were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), N2 adsorption-desorption test. Meanwhile, the results of electrocatalytic oxygen evolution reaction for the flake Co9S8/ZnS/C composite showed that it had high electrocatalytic oxygen production performance, with the initial overpotential of 390 mV and the Tafel slope of 144 mV·dec-1. |
Keywords: Co9S8/C ZnS transition metal water splitting oxygen evolution reaction solvothermal method |
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LI Zhi-Xue,REN Tie-Qiang,GENG Zhong-Xing,YANG Zhan-Xu.Preparation and Electrocatalytic Performance of Flake Co9S8/ZnS/C Composites for Oxygen Evolution Reduction[J].Chinese Journal of Inorganic Chemistry,2019,35(12):2318-2322. |
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