水热法合成MCM-41分子筛时添加辅助烃的影响
SYNTHESIS MESOPOROUS MOLECULAR SIEVE MCM-41 IN THE SYSTEM AUXILIARY ALKANES Na2O-Al2O3-SiO2-CTAB-H2O AND THEIR PROPERTIES
作者单位
董晋湘 太原理工大学精细化学研究所太原 030024 
徐红 太原理工大学精细化学研究所太原 030024 
刘光焕 太原理工大学精细化学研究所太原 030024 
高振起 太原理工大学精细化学研究所太原 030024 
吴锋 北京理工大学材料与化学工程学院北京 100081 
摘要: 
关键词: MCM-41 水热合成 辅助烃 表征
基金项目: 
Abstract: By using cetyltrimethylammonium bromite (CTAB) as template, influences of auxiliary alkanes (n-hexane, n-heptane, iso-octane, and petroleum ether) for synthesizing mesoprours molecular sieve MCM-41 with more than 4 nm pore have studied in hydrothermal system. It was proved by experiments that molecular sieve MCM-41 with d100>4 nm could be obtained with putting auxiliary alkanes. As-synthesized samples have been characterized by XRD, SEM and N2 adsorption. The experimental results showed that adding auxiliary alkanes made decreasing order of molecular sieve MCM-41.
Keywords: molecular sieve MCM-41 synthesis auxiliary alkanes characterization
 
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董晋湘,徐红,刘光焕,高振起,吴锋.水热法合成MCM-41分子筛时添加辅助烃的影响[J].无机化学学报,1999,15(1):104-109.
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