钛氧有机化合物常压低温液相合成纳米二氧化钛晶体的研究 |
Study on Synthesis of Nanometer TiO2 Crystal from Titanyl Organic Compound in Liquid Phase at Normal Pressure and Low Temperature |
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摘要: |
关键词: 纳米粒子 二氧化钛 钛氧有机化合物 液相合成 |
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Abstract: FTIR and NMR results show that a majority of the solid product prepared from the reaction of Ti(OC4H9)4 and excessive (CH3CO)2O is titanyl acetoxyl [TiO(OOCCH3)2]. The particle size, shape and forming process of the crystal were studied with XRD and TEM. The specific area data of a rutile TiO2 sample and the powders obtained after calcination at different temperatures have been measured with BET method. |
Keywords: nanometer particle TiO2 titanyl organic compound synthesis in liquid phase |
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陈小泉,古国榜.钛氧有机化合物常压低温液相合成纳米二氧化钛晶体的研究[J].无机化学学报,2002,18(7):749-752. |
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