| o-ZrW1.6Mo0.4O8·H2O正交相的合成与表征 |
| The Preparation and Characterization of Orthorhombic o-ZrW1.6Mo0.4O8·H2O |
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| 摘要: |
| 关键词: ZrW1.6Mo0.4O8·H2O 合成 表征 |
| 基金项目: |
| Abstract: The precursor ZrW1.6Mo0.4O7(OH)2(H2O)2 was characterized by IR and XRD methods. δ′-ZrW1.6Mo0.4O8 was prepared by careful controlling the annealing conditions from the precursor and was determined to have the formula as o-ZrW1.6Mo0.4O8·H2O by TG-DSC, IR, and XRD methods. The relation between o-ZrW1.6Mo0.4O8·H2O and o-ZrW1.6Mo0.4O8 was discussed through variable temperature XRD patterns. Further more, the mechanism of the precursor dehydration was suggested. |
| Keywords: ZrW1.6Mo0.4O8·H2O preparation characterization |
| 投稿时间：2005-03-06 修订日期：2005-05-23 |
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| 黄令,刘鹏辉,马辉,齐传民,赵新华.o-ZrW1.6Mo0.4O8·H2O正交相的合成与表征[J].无机化学学报,2005,21(10):1531-1534. |
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