烷烃溶剂热法合成单分散硒化锌准纳米球
Synthesis of Monodispersed ZnSe Quasi-nanospheres by Hydrocarbon Solvothermal Method
作者单位
陈 渊 北京大学应用化学系北京 100871
中信国安盟固利新能源科技有限公司北京 102200 
冯华君 北京大学应用化学系北京 100871
中信国安盟固利新能源科技有限公司北京 102200 
其 鲁 北京大学应用化学系北京 100871
中信国安盟固利新能源科技有限公司北京 102200 
张敬华 中信国安盟固利新能源科技有限公司北京 102200 
摘要: 
关键词: 烷烃溶剂热  金属硒化物  单分散纳米球
基金项目: 
Abstract: Monodispersed ZnSe quasi-nanospheres have been prepared by a hydrocarbon solvothermal route at 180℃ using decahydronaphthalene, zinc stearate and selenium as starting materials. The as-obtained products were characterized by SEM, TEM, XRD, elemental analysis and electron-diffraction techniques. Electron microscopy reveals that ZnSe particles prepared in decahydronaphthalene are monodispersed with an average particle size of 55 nm. The possible formation mechanism was investigated by changing hydrocarbon solvent. The shape and size of ZnSe particles depend on the structure of hydrocarbon solvent.
Keywords: Hydrocarbon solvothermal  Metal selenide  Monodispersed nanospheres
 
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陈 渊,冯华君,其 鲁,张敬华.烷烃溶剂热法合成单分散硒化锌准纳米球[J].无机化学学报,2008,24(7):1177-1181.
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